Xin-Ying Li, Mei Yang, Jie-Yun Huang, Xiao-Xue Yu, Min-Qian Zhao, Zhi-Kun Liang, Zhi-Sheng Xie, Xin-Jun Xu. Preparative separation and purification of deoxyschizandrin from Schisandrae Sphenantherae Fructus by high-speed counter-current chromatography[J]. Journal of Pharmaceutical Analysis, 2013, (6): 429-433.
Citation:
Xin-Ying Li, Mei Yang, Jie-Yun Huang, Xiao-Xue Yu, Min-Qian Zhao, Zhi-Kun Liang, Zhi-Sheng Xie, Xin-Jun Xu. Preparative separation and purification of deoxyschizandrin from Schisandrae Sphenantherae Fructus by high-speed counter-current chromatography[J]. Journal of Pharmaceutical Analysis , 2013, (6): 429-433.
Xin-Ying Li, Mei Yang, Jie-Yun Huang, Xiao-Xue Yu, Min-Qian Zhao, Zhi-Kun Liang, Zhi-Sheng Xie, Xin-Jun Xu. Preparative separation and purification of deoxyschizandrin from Schisandrae Sphenantherae Fructus by high-speed counter-current chromatography[J]. Journal of Pharmaceutical Analysis, 2013, (6): 429-433.
Citation:
Xin-Ying Li, Mei Yang, Jie-Yun Huang, Xiao-Xue Yu, Min-Qian Zhao, Zhi-Kun Liang, Zhi-Sheng Xie, Xin-Jun Xu. Preparative separation and purification of deoxyschizandrin from Schisandrae Sphenantherae Fructus by high-speed counter-current chromatography[J]. Journal of Pharmaceutical Analysis , 2013, (6): 429-433.
Preparative separation and purification of deoxyschizandrin from Schisandrae Sphenantherae Fructus by high-speed counter-current chromatography
School of Pharmaceutical Sciences, Sun Yat-Sen University, No. 132, East Waihuan Rd., Guangzhou Higher Education Mega Center, Guangzhou 510006, China
Publish Date:
Dec. 10, 2013
Abstract
A high-speed counter-current chromatography (HSCCC) method was successfully developed for the preparative separation and purification of deoxyschizandrin from Schisandrae Sphenantherae Fructus in one step. The purity of deoxyschizandrin was 98.5%, and the structure was identified by MS, UV and NMR. This method was simple, fast, convenient and appropriate to prepare pure compound as reference substances for related research on Schisandrae Sphenantherae Fructus.
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