Volume 3 Issue 6
Dec.  2013
Turn off MathJax
Article Contents
Xiao-Xue Yu, Qian-Wen Wang, Xin-Jun Xu, Wei-Jian Lv, Ming-Qian Zhao, Zhi-Kun Liang. Preparative isolation of Heteroclitin D from Kadsurae Caulis using normal-phase flash chromatography[J]. Journal of Pharmaceutical Analysis, 2013, (6): 456-459.
Citation: Xiao-Xue Yu, Qian-Wen Wang, Xin-Jun Xu, Wei-Jian Lv, Ming-Qian Zhao, Zhi-Kun Liang. Preparative isolation of Heteroclitin D from Kadsurae Caulis using normal-phase flash chromatography[J]. Journal of Pharmaceutical Analysis, 2013, (6): 456-459.

Preparative isolation of Heteroclitin D from Kadsurae Caulis using normal-phase flash chromatography

Funds:

the International Scientific and Techno-logical Cooperation Program of China

the Industry-University-Research Cooperation Program from Science and Technology Department of Qingyuang City

  • Publish Date: Dec. 10, 2013
  • Heteroclitin D (H.D) was successfully isolated from Kadsurae Caulis by using flash chromatography and recrystallized by methanol, 10.2 mg of H.D was obtained from 4.86 g of crude extract, and the purity determined by HPLC was 99.4%. The structure was identified by UV, IR, MS, and NMR analysis. The fast, simple and efficient method can be applied to the preparation of reference substance of H. D.
  • loading
  • 加载中

Catalog

    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    Article Metrics

    Article views (70) PDF downloads(0) Cited by()
    Proportional views
    Related

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return