Volume 13 Issue 4
Apr.  2023
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Article Navigation >  Journal of Pharmaceutical Analysis  > 2023  >  13(4): 323-339
Xinyu Li, Qianjie Ma, Xiangtai Zheng, Qin Chen, Xiaodong Sun. Recent applications and chiral separation development based on stationary phases in open tubular capillary electrochromatography (2019-2022)[J]. Journal of Pharmaceutical Analysis, 2023, 13(4): 323-339. doi: 10.1016/j.jpha.2023.01.003
Citation: Xinyu Li, Qianjie Ma, Xiangtai Zheng, Qin Chen, Xiaodong Sun. Recent applications and chiral separation development based on stationary phases in open tubular capillary electrochromatography (2019-2022)[J]. Journal of Pharmaceutical Analysis, 2023, 13(4): 323-339. doi: 10.1016/j.jpha.2023.01.003
shu

Recent applications and chiral separation development based on stationary phases in open tubular capillary electrochromatography (2019-2022)

doi: 10.1016/j.jpha.2023.01.003

  • a. Shanghai Engineering Research Center of Organ Repair, School of Medicine, Shanghai University, Shanghai, 200444, China;

  • b. Shanghai Key Laboratory of Bio-Energy Crops, School of Life Sciences, Shanghai University, Shanghai, 200444, China;

  • c. Institute of Translational Medicine, Shanghai University, Shanghai, 200444, China

Funds:

This study was funded by the Project of National Natural Science Foundation of China (Grant No.: 82003705), and the Shanghai Science and Technology Innovation Foundation (Grant Nos.: 23010500200 and 23ZR1422700).

  • Received Date: Sep. 11, 2022
  • Accepted Date: Jan. 31, 2023
  • Rev Recd Date: Jan. 16, 2023
  • Publish Date: Feb. 06, 2023
    Abstract
  • Capillary electrochromatography (CEC) plays a significant role in chiral separation via the double separation principle, partition coefficient difference between the two phases, and electroosmotic flow-driven separation. Given the distinct properties of the inner wall stationary phase (SP), the separation ability of each SP differs from one another. Particularly, it provides large room for promising applications of open tubular capillary electrochromatography (OT-CEC). We divided the OT-CEC SPs developed over the past four years into six types: ionic liquids, nanoparticle materials, microporous materials, biomaterials, non-nanopolymers, and others, to mainly introduce their characteristics in chiral drug separation. There also added a few classic SPs that occurred within ten years as supplements to enrich the features of each SP. Additionally, we discuss their applications in metabolomics, food, cosmetics, environment, and biology as analytes in addition to chiral drugs. OT-CEC plays an increasingly significant role in chiral separation and may promote the development of capillary electrophoresis (CE) combined with other instruments in recent years, such as CE with mass spectrometry (CE/MS) and CE with ultraviolet light detector (CE/UV).
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